University of Delaware       Department of Civil & Environmental Engineering       Fall 2009

CIEG 833: Fate of Organic Pollutants in the Environment (3 credits)



OBJECTIVE:
To understand and predict the partitioning, speciation, and transformation of organic contaminants in environmental systems.  At the end of the semester, students are expected to apply the concepts and models learned to predict properties and environmental behavior of organic chemicals based on their molecular structures.
 

FORMAT:
This course is mostly lecture-based, but will also include mini-discussion sessions.  Because of the large amount of materials to cover, students are expected to complete the assigned readings before coming to class.  Each week we will discuss a specific physical-chemical property or fate process of organic chemicals, with special emphasis on the underlying principles involved.
 

CONTENTS:
The textbook consists of three main parts: partitioning, transformation, and transport.  This course will cover the first two parts only.  The first two thirds of the course will focus on the molecular properties that govern equilibrium partitioning of organic compounds among different media.  The last one third will deal with abiotic and microbial transformation reactions and the environmental agents that mediate these reactions.  We will not cover transport of organic pollutants or the case studies in the textbook.

PREREQUISITES:
CIEG632, CIEG634, CIEG636, and preferably one semester each of organic chemistry and physical chemistry (thermodynamics and kinetics).
 

TIME / PLACE:
Tuesday & Thursday, 2:00 - 3:15 p.m., DuPont 350.
 

INSTRUCTOR:
Pei Chiu, 344B DuPont Hall, 831-3104, pei@udel.edu.
 

OFFICE HOURS:
Monday 1:30 p.m. - 3:00 p.m.   You can also make appointments with me by phone or email, or simply stop by my office.
 

TEXTBOOK:
"Environmental Organic Chemistry" 2nd Ed.*, Schwarzenbach, R. P., Gschwend, P. M., and Imboden, D. M., Wiley, 2002.

*Using the first edition is discouraged.  The second edition contains a significant amount of new materials and updated information, much of which will be covered.
 

REFERENCES:
(1) Larson, R. A. & Weber, E. J. "Reaction Mechanisms in Environmental Organic Chemistry", Lewis, 1994.
(2) Brezonik, P. L. "Chemical Kinetics and Process Dynamics in Aquatic Systems", Lewis, 1994.
 

REQUIREMENTS: (200 points total)

1. Mid-Term Exam (60 points)

A mid-term exam will be held in class in late October and will cover all the materials discussed in Parts I and II of the text.  The exact time and location of the exam will be announced later.
 

2. Final Exam (80 points)

The time and location of final exam will be as scheduled by the University.  The exam will be cumulative (i.e., will cover all three Parts), although Part III (transformation) will carry more weight than Parts I and II.

3. Critical Review (60 points)

You will critically review one assigned research paper on either organic chemical partitioning or transformation.  Your review is expected to be not merely a summary of the paper but rather a critical analysis of the study, including the rationale for the research, the hypothesis(es) the author(s) set out to test, the experimental or modeling approach used, the quality of the data and data analysis, the validity of the conclusions, and the significance and implications of the findings.  It may be helpful to think about these questions: Would you have taken a different approach and why/how?  Would you analyze or interpret the data differently?  Is there an alternative or competing theory out there and, if so, do the results support the author's theory satisfactorily and convincingly?  You should take care to distinguish logical interpretation of research results from conjectures and speculations.

Your critical reviews should be between 10 and 15 pages, excluding cover page, references, and appendix.  The cover page shall include the title of the paper, course number, your name, and all the other basic information.  Use 12-point Times or Times New Roman font, double space, and 1-inch margins for all sides.  Number all pages except the cover page.  Use the Author-and-Year style for references (for example, see Applied and Environmental Microbiology).  Include citations wherever necessary, unless it is your own original contribution.  The critical review is due on Thursday, December 3rd, by 2:00 p.m. (Late Policy applies; see below).

Note — and this is important — that although most of you have written papers and reports before, I still strongly encourage you to review the Academic Dishonesty section of the Code of Conduct before you start writing.

ATTENDANCE:
Attendance is not mandatory, and no points will be deducted due to absence.  However, absence is not an acceptable reason for missing assignment deadline or exams.
 

LATE POLICY:
A late assignment (critical review) will lose 10 points per day and will not be accepted or graded after one week.
 

GRADING: Total number of points = 200.  You will need 120 points to pass.

If the total number of points you earn is greater than or equal to
170 points, you will receive an A
160 points, you will receive an A-
150 points, you will receive a B+
140 points, you will receive a B
130 points, you will receive a B-
120 points, you will receive a C
 

TENTATIVE SCHEDULE and READING ASSIGNMENTS (to be completed BEFORE class):

1.        Scope, objectives, and house-keeping details.
           Overview of organic chemicals in environments.  Review of basic concepts in organic chemistry.
           Reading Assignment: Chapters 1 and 2.

2.        Principles of organic partitioning: Molecular interactions and thermodynamics.
           Reading Assignment: Chapter 3.

3.        Vapor pressures, activity coefficients, and water solubility of organic compounds.
           Reading Assignment: Chapters 4 and 5.

4.        Partitioning: air—water, air—organic solvent, and organic solvent—water.
           Reading Assignment: Chapters 6 and 7.

5.        Organic acids and bases.
           Reading Assignment: Chapter 8.

6.        Sorption of organic solutes to natural organic matter.
           Reading Assignment: Chapter 9.

7.        Partitioning of organic solutes into living organisms.
           Reading Assignment: Chapter 10.

8.        Sorption of nitroaromatics to inorganic surfaces.
           Reading Assignment: Section 11.3.

9.        Thermodynamics and kinetics of transformation.
           Reading Assignment: Chapter 12.

10.      Non-redox reactions: nucleophilic substitution and elimination.
           Reading Assignment: Chapter 13.

11.      Abiotic oxidation-reduction (redox) reactions.
           Reading Assignment: Chapter 14.

12.      Microbial and enzymatic tranformation.
           Reading Assignment: Chapter 17.

13.      Direct photolysis.
           Reading Assignment: Chapter 15.

14.      Indirect photolysis.
           Reading Assignment: Chapter 16.

15.      Review and Q/A.  Concluding remarks and feedback.  Course evaluation.


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